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Brinell Hardness Testing 101

What are the most desirable attributes of a Brinell hardness tester? Does it belong in your heat treat department? Read this equipment overview to decide. 

Read the English translation of this article in the version below or read the Spanish translation when you click the flag to the right. Both the Spanish and the English versions were originally published in Heat Treat Today's August 2023 Automotive Heat Treat print edition.


Alex Austin
Managing Director
Foundrax Engineering Products Ltd
Source: Foundrax

All heat treatment companies must test hardness; many with a Brinell tester. Existing since 1900, a review of this time-tested method is in order.

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The Brinell test requires a tungsten carbide ball indenter to be forced vertically into the surface of the test material, placed on a rigid anvil. The diameter of the indentation made by the ball is then measured across both its x and y axes as a minimum, and the average of these measurements is taken as the working figure. The technician can then either feed that figure into an equation to determine the hardness or read from a “diameter-to-hardness” chart.

There are various forces and indenter diameters available for Brinell testing reflecting the very wide range of metals that need to be assessed, but most tests involve a 10 mm ball under a 3,000 kg load. In large, floor standing machines, the indenter is usually motor-driven, but some machines use levers and weights, while others are hydraulic or pneumatic. The Brinell test remains the default method for hardness measurement in many heat treatment facilities, for three primary reasons.

1.  Surface Preparation

Preparing the surface of a sample for Brinell testing takes just a few seconds with a grinder. Provided the sample is sitting steadily on the anvil and the top face of the sample is perpendicular to the direction of force of the indenter — as mandated by the standards — the surface does not need to be particularly smooth.

Figure 1. Heavy-duty Brinell tester in situ

2. Surface Contamination

Minute surface contaminants under a Brinell indenter are unlikely to cause a “mis-test.” By comparison, during Rockwell testing, the most widely used method across all industries, a tiny diamond indenter penetrates the surface by less than one hundredth of an inch, and any contaminants or surface abnormalities (including parallelism) that could impede or assist the progress of the indenter are a problem, which means that Rockwell samples must be carefully prepared before testing.

3. Portable

Perhaps most significant, rugged, hand-held portable Brinell testers with hydraulic test heads enable large, heavy, and awkwardly shaped components of rough surface finish to be tested in situ. This feature is of such utility in industry that the international standards authorities give a dispensation — a special designation — to portable machines, although their performance cannot be directly verified like their floor-standing cousins.

With forces ranging from 3000 kg down to 1 kg and indenter balls as small as 1 mm, Brinell testing can be used on a vast range of metal, but forges, foundries, heat treatment plants, quality control areas, and laboratories are the places one would most likely find a test machine working at 10 mm/3000 kg. It was mentioned earlier that the surface of test samples doesn’t need to be particularly smooth, in fact roughly- ground surfaces on materials with a coarse grain structure can be measured quite safely because the diameter of the indentation is so large relative to any irregularities on the surface.

Figure 2. Close-up of a calibration-grade Brinell tester

In Figure 2, a calibration-grade Brinell tester drives the tungsten carbide ball into the test sample. The ball is being held in position to stabilize plastic deformation. ASTM E-10 and ISO 6506 — the authoritative documents for Brinell testing — lay out standards in detail, but the practical procedure for workshop technicians is very straightforward; training should not take longer than an hour. When testing forgings, billets, and other samples, one indentation should suffice but in certain critical applications more than one indentation may be used for assurance.

The question of whether to test every sample in a batch will depend on how inconsistent those samples might be; it has nothing to do with any issues with Brinell testing itself. In certain industries, every single product is tested because the risk of failure is too high. A good example of this is the production of links for the tracks used on tanks and other armored vehicles. Every link in every tank track in use by the British Army has been Brinell tested on a high-speed, fully automatic machine that features a powerful integral clamp to keep the component rigid during the test. You can view the machine in Figure 1 on page 44. Subject to reasonable care, a heavy-duty Brinell tester will perform many hundreds of thousands of tests. The machine in Figure 1 has performed several million.

Tests take approximately fifteen seconds. The indenter must be driven uniformly into the material with no possibility of either a rebound or a speed that would “punch” the indenter into the material. Also, the metal must be loaded for a sufficient length of time to ensure the indentation is properly (plasticly) deformed, that is, the risk of an indentation shrinking very, very slightly after the indenter is withdrawn is kept to a minimum.

Figure 3. Measurement of Brinell hardness test indentation

Measuring the indentation is more challenging. After carefully making the indentation and withdrawing the test sample from the “jaws” of the test machine, one must measure the indentation across at least two diameters. Given that Brinell indentations are at most 6 mm across and that 0.2 mm difference in diameter might equal 20 hardness points, getting the measurement right is critical — and tricky. Most technicians will use an illuminated microscope to do this, but even then it can be a challenge. Consider Figure 3 on the next page.

Making an indentation leaves a “ridge” at the indentation perimeter because metal is not just pushed downwards, but also sideways. This ridge can obscure where the real indentation begins, and three different technicians can easily make three different estimates of where that is. And this variation in operators’ interpretation of results is why, for over 80 years, the Brinell test was seen as a little “rough and ready,” for the workshop machinist, perhaps, but probably not for the laboratory scientist.

Manual measurement microscopes have improved over the years, and a relatively “clean edged” indentation with a crisply illuminated graticule can be less challenging for the experienced technician to make an accurate measurement. Figure 4 is a less difficult scenario than the one above. Even so, how can we know if we have really judged the position of the edge precisely?

Figure 4. Measurement with improved microscope and well-illuminated graticule

In 1982, the first automatic reader hit the markets. This was the culmination of years of research and used proprietary software that pushed the computers of the day to their limits. The equipment could make hundreds of measurements across the indentation and calculate the mean diameter in a split second. Not long afterwards, it was available as an integral part of a Brinell test machine. Word of this equipment soon reached critical users in the oil tool industry, and they mandated its use to their suppliers. Within 15 years, the use of this technology was widespread and the perception of the Brinell test’s accuracy had been transformed. The Brinell test, in a sense, had come of age. See Figure 5 for the latest version of that automatic microscope in action.

Finally, like any important measuring equipment, regular calibration and servicing is desirable, if not compulsory. Manufacturers typically stipulate a service schedule which must be considered alongside the calibration rules dictated by international agencies.

When considering options for hardness testing of heat treated samples, there are ultimately three test methods: Brinell, Rockwell, and Microhardness (Vickers or Knoop).

Figure 5. Latest version of the automatic microscope in action

While Brinell testing isn’t suited to very small or very thin samples, it is relatively “immune” to small contaminants, the indenters are not expensive, and the width of the indentation means that testing of coarse grained and roughly finished surfaces is not problematic. With the development of reliable automatic indentation measurement, the one serious deficiency of the Brinell test was overcome, providing the assurance that was vital to critical components suppliers in all types of industries such as oil and gas, aerospace, defense, and transportation.

About the Author:

Alex Austin has been the managing director of Foundrax Engineering Products Ltd. since 2002. Foundrax has supplied Brinell hardness testing equipment since 1948 and is the only company in the world to truly specialize in this field. Alex sits on the ISE/101/05 Indentation Hardness Testing Committee at the British Standards Institution. He has been part of the British delegation to the International Standards Organization advising on the development of the standard ISO 6506 “Metallic materials – Brinell hardness test” and is the chairman and convenor for the current ISO revision of the standard.

For more information:
Contact www.foundrax.co/uk.


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Meet the Consultant: Dan Kay

The brain drain is real. As new professionals enter the industry, Heat Treat Today is helping to ensure that young and old inquiring minds can connect with and grow from the experiences of high-value industry experts. Get to know the first Heat Treat Today Consultant: Dan Kay.


Daniel Kay
Owner
Kay & Associates

I am Dan Kay (which is a shortened form of my birth name: William Daniel Kay). Although I was born in Ohio, I grew up in New Jersey, went to college (Rensselaer Polytechnic Institute) in New York State, and graduated with a degree in Metallurgical Engineering. I grew up in a wonderful family, as the third child out of six children that my parents had. They were both strong spiritual leaders, too, shaping our Christian faith and helping us to make it a strong foundation in our lives. I am married to a wonderful woman, and we’ll be celebrating our 55th wedding anniversary together in June. She continues to be a real blessing to me in so many ways. My home is in Simsbury, CT, where we have now lived for the past 25 years

Dan Kay lectures at one of his popular seminars on brazing.
Source: Kay & Associates

Dan Kay’s biggest strength is teaching and training. Being able to effectively communicate to others, verbally and in writing, to bring about positive change in others is not easy in today’s world, but it is something Dan believes he has learned to do well. Currently, Dan uses his teaching skills at brazing seminars that help to increase productivity and reduce scrap and rework.

For almost 60 years, Dan has been involved in the heat treating industry. His specialty is brazing: the joining of metal parts together to form complex assemblies, using a brazing filler metal (BFM) that melts and flows by capillary action into joints between the component parts making up that complex assembly. Out of these 60 years, Dan has many stories, but one stands out: discovering the cause of a mushy joint in tweezers used in the medical industry. After carefully studying the manufacturer’s operations, Dan suggested waiting several seconds after brazing by induction heating and before quenching, allowing the filler metal to solidify completely. After this, the tweezers no longer broke when doctors used them to stitch up patients.

Dan Kay's biggest strength is teaching and training.
Source: Kay & Associates

In Dan’s opinion, brazing and heat treating need to form a stronger partnership in the years ahead. Increasingly more metals require heat treating to obtain optimal properties for end-use service conditions. Brazing is also a growing industry, enabling more and more complex parts to be created, many of which need enhanced properties for successful use in the field. This will typically require more and more vacuum brazing/heat treat to be done, and heat treat personnel need to become familiar with brazing and its requirements, so that mistakes will not occur. Vacuum furnaces need to have additional complex internal heat treat and quench capabilities for a wide variety of metals, including aluminum, to allow such parts to be brazed, and then heat treated and quenched in multi-bar furnaces.

To learn more from Dan, visit his website kaybrazing.com/seminars to attend his next seminar


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Potential for L-PBI Titanium Alloy in Aero and Medical Industries

Source: TAV Vacuum Furnaces 

Those familiar with vacuum heat treatments are surely acquainted with the vacuum heat treatment of titanium and how such furnaces create the ideal environment for titanium's heat treatment. However, not all titanium and its alloys are created equal. Enter the beta titanium alloy.

In this best of the web article from TAV Vacuum Furnaces, discover the potential applications for beta titanium alloys, as well as the effects that various vacuum heat treatments can have on the mechanical properties of the alloy. Additive manufacturing (AM) technologies, specifically laser powder bed fusion, are gaining increased interest in the treatment of beta titanium alloys, due to their efficiency and their cost-cutting potential. Learn more about the chemistry and applications of this unique material below.

An excerpt:

Beta titanium alloys have an unique combination of desirable properties: their high specific strengths, creep resistance, oxidation and corrosion resistance, excellent temperature resistance up to 600°C and hardenability, make them very attractive for aerospace applications. On the other hand, the excellent biocompatibility and low elastic modulus, closer to that of human bone compared to other alloys, make Ti beta alloys an excellent material for biomedical applications.

Read more: "Vacuum Heat Treatment of L-PBF Beta Titanium Alloys-TAV Vacuum Furnaces at ECHT 2023”


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Women’s Roundtable: Leadership in Heat Treat

For this release from our September print edition, specifically concerned with the different “People of Heat Treat,” Heat Treat Today was curious what a group of distinguished women taking the lead in North America’s heat treat industry had to say about their experiences in a space where women are the minority. Hear a bit of their personal stories of challenge and success in the roundtable below.

This article originally appears in Heat Treat Today's September 2023 The People of Heat Treat print edition.


1. What is your “origin story” of entering the
heat treat industry?

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Deidra Minerd, Operations Manager & Metallurgical/Process Engineer, The Euclid Heat Treating Company: I entered the heat treating industry because it was a family business. That wasn’t my original plan, though, as I started my college career in pharmacy. Summer jobs were at the family heat treating business that my grandfather started, and one summer I decided to change schools and study metallurgical engineering, with the intent to join the business after college.

Debra James, President/CEO at METALEX THERMAL SPECIALTIES: I began working for a company that did ion nitriding in 2012. I was hired as the office administrator, but it was a small company, so we wore many hats that included helping the guys in the shop loading and unloading parts when they needed a hand. From there, it was a learning process of understanding the heat treating industry, working with customers to meet their expectations, and developing business relationships.

The gentleman that owned the company was a great mentor who encouraged growth and development. He wanted me to purchase the company, and we had started down that path when he passed away. In 2019, his successors took over the company, but they did not focus on customer service, growing the company, or making improvements.

Debra James, President/CEO of METALEX (Source: METALEX)

That is when we began looking for an outside company to purchase. We were able to purchase a small heat treating company in Berthoud, Colorado. Immediately, we took steps to focus on customer service and offering updated processes to our customers. We have received very good feedback from our customers, and we have been able to grow our sales by 20% each year. We also took steps to get our Women’s Business Enterprise National Council (WBENC) certification, as well as our AS9100 certification. In addition, we were able to relocate the business to a much larger facility that will enable us to continue to grow and expand.

Mary Springer, Executive Vice President at ThermTech Of Waukesha, Inc: In 1968, my dad started his own heat treating company called Midland Metal Treating in Franklin, WI. I was 10 years old. He had worked as a tool and die heat treater at Simmons Company, and other places. He was very proud of his heat treat journeymen’s card.

Midland was very much a family endeavor. There were four of us and we all went to work with dad, mostly to spend time with him. I became an expert at running the induction hardening department. I was a tomboy, so I loved the shop environment. I worked as much as I could, in the beginning for root beer and Cheetos! However, spending hours and hours pushing a button and watching a part heat up became pretty monotonous.

My dad never dissuaded me from working with him, but I got the sense that he wanted me to go to college, yet the subject of engineering never really came up. I wanted to be an oceanographer and follow Jaques Cousteau around the globe, but found that I really did not want to leave my family. So, I ended up with several of my friends in nursing school, working for dad in the summer.

After obtaining a master’s degree in Nursing and a minor in Business Management, I worked as a nurse educator for a large hospital system and taught at the local university. In the late 1970s, the recession took its toll on Midland, and my dad had sold the company under duress.

A year later, at the age of 54, he decided to roll the dice again and started ThermTech. My brother was studying metallurgy at UW-Madison, and my older sister was working in the office. I felt a longing to be a part of it again. In 1987, I left my job at the hospital and joined my dad and siblings. Everyone did everything they could to make a go of it and little by little, we grew ThermTech. I kept a job working weekends as a home IV oncology nurse until 2004, as I did miss my old job!

As ThermTech grew, my older sister left, and my brother and I learned to work together sharing the duties of running a business. My dad retired when he was 70, and my brother and I became equal stock owners.

2. Have there been any challenges that you’ve
encountered in heat treat? 

Mary Springer received MTI’s Heritage Award in 2019, an award which recognizes an individual’s lifetime commitment to the betterment of the commercial heat treating industry. (Source: MTI)

Deidra Minerd: One challenge I faced when I started was translating what I learned in college to what was happening on the shop floor. I had a lot of book knowledge, but I didn’t know how to run a heat treating furnace. I had to make the effort to learn from people on the shop floor, ask questions (even if they sounded like stupid questions), and get my hands dirty so I could learn and earn their respect.

Debra James: Occasionally I encounter people who do not think women really belong in the heat treating industry and assume that I am just an employee rather than an owner of the business. The other major hurdle that we have encountered is getting financing for equipment. Our equipment purchases are usually used equipment due to the prohibitive costs of new equipment and being able to access financing for used equipment can be difficult.

Mary Springer: Heat treating is VERY challenging. Different problems every day. That is what I love about it. I work hard to develop relationships with employees. Currently, we employ 155 people, we run 3 shifts 24 hours/6 days a week. I love planning expansion, figuring out financing on large projects, and solving problems.

3. What solidified your leadership in this industry?

Deidra Minerd: While I certainly don’t feel like an expert, I’m reminded every now and then that I have certainly collected quite a bit of expertise over the years. An important lesson I learned, however, is that having the most technical knowledge does not necessarily make you the best leader. There is an additional set of skills necessary to successfully lead a group of people and/or a business, and that set includes humility, patience, integrity, good communication skills, and the ability to see the big picture and be open to change. Years ago, my mentor, Roger Fabian, suggested that I would be a good leader in my company, and that was an important moment for me. He had been a leader in the heat treating industry, and I valued his opinion and appreciated that he noticed that in me.

Debra James: The key factor that solidified my desire to own our heat treating business was first the support and encouragement that I had received from the gentleman that originally owned the ion nitriding company I worked for. He was a very knowledgeable person and knowing that he thought I could run my own heat treating business made me see that possibility. In addition, knowing that I could do a better job of owning, managing, and operating a company than the successors that took over his business was also a motivating factor.

Mary Springer: As a company, the realization that my brother and I have built a “brand” in the industry, watching our sales/profit grow, and knowing how proud our mom and dad would be of what we did with the great opportunity they afforded us . . . feels very nice. Also, we each have a son in the business, and they are coming into their own, hearing their ideas for the future . . . exciting! I guess I do not consider myself an expert in the industry, only someone who is hardworking and always curious!

4. Any advice you’d give to women in heat treat to enjoy and “own” their position?

Deidra Minerd receiving Distinguished Service Award in 2018.

Deidra Minerd: My advice to women would be to “own” their knowledge and be confident in it, but also be willing to ask questions. I think young people may be hesitant to say they don’t know something, for fear of not being perceived as “smart.” However, a lot of knowledge is gained from peers instead of from books, so the ability to constantly learn is important.

Debra James: First of all, embrace this industry and realize all that there is to learn. Always be looking at ways to improve what you do and how you can best meet your customer’s needs. Establish yourself as the person the customer/contact needs to talk to.

Mary Springer: For me this has never been about being a “woman in a man’s world.” I have never experienced anything but acceptance in this industry. Working hard is working hard. If you put your best effort forward, you will enjoy the fruits of that effort. Dedication earns respect, there’s no other way around it. Never stop learning, and remember, no one can “have it all.” Choices have consequences, good and not so good. But never complain about the consequences of your choices, you have to own it. Don’t do it if you don’t love it!

5. What is the best part of the heat treat industry?

Deidra Minerd: What I love about heat treating is the history and consistency of metallurgy. You can have a very fancy furnace that follows a program minute-by-minute with thermocouples to monitor the temperature of the part, or you could heat it up in an open-fire furnace and quench it with tongs in a 5 gallon bucket of oil, and it will respond the same way. New technology doesn’t change the basics of metallurgy.

Debra James: The best part of the industry is that there is always something to learn and new avenues to explore for growth and development of yourself personally and professionally. I truly enjoy our customers and the relationships that we have built with them. It is so rewarding when they tell us how much they appreciate what we do for them.

Mary Springer: In commercial heat treating, I find it very challenging to anticipate the needs of our regional market, to be able to reinvent ourselves technically to serve new demands. It is exciting to bring new equipment in and see the growth. I love to see our people grow and learn, prosper from their careers here. We have many people with over 15 years’ experience. Figuring out how to connect with the younger generation has been a journey . . . . Also, it is always interesting, but difficult to learn from mistakes. Surviving whatever! I remember in late 2019, my sales manager came in one day and said, “Do we have a plan for a pandemic? There is this COVID thing going on in China . . .” I kind of chuckled and said, “It’s just the flu!!!!” HA! You just never know where the next challenge will come from. Try always to keep a light heart.

About the Industry Leaders

Deidra Minerd is the Operations Manager & Metallurgical/Process Engineer at The Euclid Heat Treating Company.

Debra James is the president/CEO at METALEX THERMAL SPECIALTIES.

Mary Springer is the Executive Vice President at ThermTech of Waukesha, Inc.


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Heat Treat Boot Camp Year #2 in the Books!

Another Heat Treat Boot Camp has come and gone. Yesterday marked the end of a successful second year in Pittsburgh, Pennsylvania. This intensive basic training for the heat treat industry had attendees networking, gaining new practical knowledge, and getting their "boots" on the ground and up Pittsburgh's Duquesne Incline and Penna Flame's flame hardening plant.

The event opened on a Steelers vs. Browns Monday, September 18, where the trainees got to know one another over food and drink at a reception. Seven sessions ensued between Tuesday, September 19, and Wednesday, September 20. Instructors Doug Glenn, publisher and founder of Heat Treat Today, and Thomas Wingens, president/CEO and founder of WINGENS International Industry Consultancy took these two days to bring the 40+ trainees up-to-speed on "Heat Treat Players," "Latest Heat Treat Developments," and more. Questions and discussion were encouraged during the formal sessions, and heat treaters had plenty of informal, additional learning time through interactions with each other and the instructors.

Highlights of the Event

“We had substantial growth of the number of people here, about a 33% increase [in attendance from last year]. We had over 40 people that attended, and the interaction was really remarkable," commented Glenn. He added, "One of the best benefits we had was the networking that went on. The presentations were good, we even made improvements over last year. I’m very, very pleased with the results; I think it was a great event."

At the end of the first day of lectures, nearly all of the attendees boarded a rented school bus to visit the Duquesne Incline on Mount Washington and enjoy the view of Pittsburgh. Following another day packed with training and resources, attendees had the option to visit the Penna Flame to check out the flame hardening services. Over half of the attendees ventured out to the Zelienople-based plant, applying what they learned about heat treat processes, parts, and markets that had been discussed during lectures. Andrew Orr, vice president at Penna Flame, gave the group a first-class tour of the facility to witness induction hardening, collaborative robots, quenching, and flame hardening in action.

Attendees gathered on the last day of lectures for a final picture. Doug Glenn, publisher of Heat Treat Today, is pictured second row back on the far left. Thomas Wingens, WINGENS LLC, stands second row back on the far right.

Heat Treat Today thanks everyone for their participation in this amazing year #2 Heat Treat Boot Camp. Plans are underway for Heat Treat Boot Camp 2024. Stay tuned for registration information; see you next year!

Photo Source: Heat Treat Today


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Nitrex and Linde

Nitrex and Linde announced they have renewed and expanded their heat-treating focused joint marketing agreement. What started as a local agreement 13 years ago, between Nitrex and Linde, formerly known as UPC-Marathon and Praxair, respectively, has evolved into an international marketing agreement and now covers Europe and North America.

To date, Nitrex and Linde have worked together on over 30 projects. By using their complementary offerings, they have upgraded essential equipment and have helped customers achieve quality results. Nitrex provides Linde customers with equipment and analyses to control first-rate gas atmospheres, thanks to its competence in the heat treatment and electrical fields, technical solutions, support, and world-class gas panels.

“Our competencies complement each other,” says Roman Grosman, National Director of Business Development for Linde in the U.S.  “In the event that Linde’s heat treatment clients require equipment that we do not offer, Nitrex can meet this need.”

“This continues to be a win-win relationship,” says Paul Oleszkiewicz, President, CPO & CSO of UPC-Marathon, a Nitrex company. “We can supply Linde gas customers with process controls, and in turn, Linde offers a reliable gas supply network. We are both aiming for the highest quality, efficiency, performance, and a greener tomorrow and providing optimal service for our customers.”


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GKN Aerospace Expands with 2 New AM Systems

GKN Aerospace has expanded its capabilities with additive manufacturing (AM) machines, accelerating its industrialization of sustainable aero engine solutions. This new technology will offer more reliable and sustainable alternatives to traditional castings and forgings.

The supplier of these machines is Nikon SLM Solutions, whose NXG XII 600's printing area and 12 lasers align with GKN Aerospace's vision to produce large parts with high productivity. Two systems have been ordered, one to be used with In718 and another for Ti64.

In the words of Martin Thordén, VP of Permanova, the newly formed business unit for material solutions within GKN Aerospace, "Partnering with Nikon SLM Solutions is a key milestone in our journey to create better, more sustainable aerospace products. . . . This collaboration provides us access to cutting-edge additive manufacturing capabilities necessary to propel us towards our net zero ambition."

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Optimize Working Life and Performance of Heat Treatment Alloy Castings

When it comes to optimizing the working life and overall performance of heat treatment alloy castings, proper alloy selection and design based on the intended application is a critical starting point. Discover the variables behind alloy selection and design and the additional factors that contribute: furnace maintenance, casting inspection, and cost reduction strategies.

This Technical Tuesday article was composed by Matthew Fischer, manager of Technical Sales, Castalloy Group for Heat Treat Today's August 2023 Automotive Heat Treating print edition.


Alloy Selection and Design Criteria 

Matthew Fischer
Manager of Technical Sales for Heat Resistant Products
Castalloy Group NA
Source: Castalloy Group

Optimal design and alloy composition for any heat treatment casting always requires careful consideration of a number of key operating variables. This is the only way to guarantee the part will deliver maximum utilization and efficiency for the intended application.

These variables include:

  • Anticipated service and maximum operating temperature
  • Size, orientation, and weight of the load
  • Thermal cycling and/or quenching
  • Range of temperature cycling
  • Frequency of temperature cycling
  • Rate of change of temperature
  • Type of atmosphere or other corrosive conditions of the application
  • Type of quenching or cooling
  • Size, shape, and weight of part(s)
  • How are the parts loaded and oriented? (e.g., manually, robotically, individually, bulk)
  • How is the alloy supported in the equipment? (e.g., rails, hearth, rollers, piers)
  • Additional processing requirements (e.g., machining, welding)
  • Abrasive or wear conditions
  • Ease of use (ergonomics) and replacement
  • Cost — initial and total cost of ownership

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In addition, there are fundamental factors that heavily influence optimal component design and alloy composition. For instance, the type of furnace used (e.g., box, pit, integral quench, continuous), alloy handling mechanism (fixture and tray), and application process (e.g., carburizing, normalizing, annealing, austempering, vacuum heat treating) all have an important role to play. It is worth noting, however, that the decision-making process is a fine balancing act that isn’t necessarily evenly weighted. While a specific alloy composition may Fiaddress the majority of performance needs, it may hinder others. Prioritizing end-use performance traits is therefore essential.

Furnace and Process Environment Maintenance 

Figure 1. Cast tray and fixtures
Source: Castalloy Group

How furnaces and processes are performance monitored and maintained is also key when seeking to optimize the performance and lifespan of heat treatment alloy castings. The specific type of furnace will dictate exact equipment and process maintenance requirements, but there are several universal best practice procedures and guidance processes that should be followed.

For instance, the Automotive Industry Action Group (AIAG) has established CQI-9 (Continuous Quality Improvement) standards for heat treatment. These standards provide the guidelines for a continuous cycle of assessment, planning, and improvement with respect to heat treat processing and due care of handling customer parts. The CQI-9 standards direct the heat treater to have and maintain the necessary equipment and associated control instruments used to monitor and record the furnace process operating parameters. They also promote the proper furnace operating process environment. However, the standards do not comprehensively address the overall maintenance requirements of the furnace and process environment equipment. Generally, yearly scheduled maintenance is important to the long-term successful continuous operation of furnace equipment. Lack of or intermittent maintenance can lead to unplanned shutdowns. Here are some of the most common maintenance issues to monitor and remedy:

Example 1: Support Misalignment

If base tray support mechanisms are in alignment (in the direction of travel) and flat (level throughout) to provide proper support of the base tray and associated fixtures and parts, then the tray should move through the furnace equipment without issue, provided the tray is in good operating condition. However, if there are broken rails or piers — or broken/deformed roller rails or wheels — then over time the tray may exhibit wear, deformation, cracks, or breaks.

Example 2: Transfer Mechanism Misalignment

If the transfer mechanisms are square to the tray (in the direction of travel) and level throughout, providing proper contact with the base tray, then the tray should move through the furnace equipment without issues, provided the tray is in good operating condition. However, if there are misaligned transfer mechanisms (pusher rods, pusher head, handler head etc.), then over time the tray may exhibit associated wear, deformation, distortion, cracks, or breaks.

Figure 2. Flat level surface and tray/grid
Source: Castalloy Group

Example 3: Uneven Heating

Although the furnace may be able to maintain an average furnace temperature as measured by a single control thermocouple, there may be uneven heating conditions (side-to-side, top-to-bottom, front-to back) due to a variety of factors, which could result in uneven thermal cycling of the alloy castings. This potential non-uniform heating of the alloy could lead to deformation, cracks, or breaks of the alloy castings. The CQI-9 standards work to monitor and address non-uniform heating using a periodic temperature uniformity survey (TUS) of the furnace heating chamber.

Figure 3. Example of original supplied alloy casting for comparison.
Source: Castalloy Group

Example 4: Non-Uniform Cooling

Although the quench chamber may be able to maintain an average quench medium temperature as measured by a control thermocouple, there may be uneven cooling conditions within a load due to a variety of factors, which could result in uneven thermal cycling of the alloy castings. If left unchecked, any of these issues may result in unintended wear, deformation, distortion, cracks, or breaks of the alloy castings. Furnace material handling issues may also result in an unplanned equipment downtime and productivity loss.

Alloy Castings Inspection

Alloy castings (fixtures, trays, grids) should be inspected periodically to ensure they are in adequate working order. This inspection could be performed when the furnace equipment is taken out of operation for summer or winter maintenance inspections and shutdowns. The main areas to consider are flatness, squareness, and proper proportion.

Damaged component
Source: Castalloy Group

Flatness

Trays, grids, and fixtures should remain flat or level across the width and length. Sagging, bowing, warping, or twisting can cause material handling issues within furnaces and associated process equipment. A simple method to check the flatness is to have a table with a flat and level surface where the tray, grid, or fixture may be placed to check and observe the flatness of the alloy casting. An alternate method to check the alloy casting flatness would be to use a level across the casting to check flatness.

Squareness

Trays, grids, and fixtures should remain square across the width and length. Being out of square can cause material handling issues within furnaces and associated process equipment. A simple method to check the squareness is to have carpenter’s square tool where the tray, grid, or fixture may be examined to observe the squareness of the alloy casting.

If the tray used in the heat treatment equipment is an assembly of trays, then each tray should be examined for squareness in all four corners. Trays that are out of square may cause tracking problems in the material handling of the furnace, or associated equipment, and should be replaced.

Figure 4. Square tool and tray/grid
Source: Castalloy Group

Proper Proportion

Trays, grids, and fixtures should remain in proper proportion as originally designed. Having bulges or large breaks that are outside of the alloy dimensional alignment compared with the originally supplied alloy casting can cause material handling issues within furnaces and associated equipment. A simple method to check the dimensional proportion is to have a picture or drawing of the originally supplied alloy casting. The tray, grid, or fixture can be compared with this in order to observe the overall soundness of the alloy casting. Suspect castings should be removed from daily operation to prevent potential material handling and associated equipment maintenance issues. An alternative to visual inspection is to make a simple jig that can be used to confirm the dimensional integrity of the alloy casting. Observable patterns of proportional changes within a common area of the alloy castings may indicate a potential issue occurring within the heat treat equipment that should be monitored and investigated before it becomes a major equipment issue and causes an unplanned equipment shutdown.

Optimizing Alloy Castings Using Periodic Purchases

Figure 5. Jig tool to check proportion
Source: Castalloy Group

Periodic purchases of alloy castings should be planned and budgeted annually to maximize casting working life, to minimize process interruptions due to potentially expired useful life of alloy castings, and to manage future expenditures for replacement alloy casting purchases.

In general, budgeting for a percentage of alloy purchases over a two to three- year period, depending on current and planned future operations, would be supportive of continuous production operations. The periodic alloy purchase is then integrated into the existing production operations and suspect alloy castings, if any, can be removed from daily production operations.

There are multiple approaches that can be implemented and adjusted according to individual plant production needs:

One approach to consider is the purchase of one-third of the total alloy purchase per year over the following three years after an initial purchase. In a continuous daily production operation, the initial purchased quantity of alloy castings will have been replaced, if needed, over the elapsed time.

An alternate approach to consider is a staggered percentage over three years. For example, 20–25% replacement the first year; 30–35% replacement the second year; 35–40% replacement the third year, adjusted as necessary based on current operating and business conditions.

This approach would also be useful for ramping up alloy quantity needs to meet increasing demand over time and could be an opportunity to address potential delivery time requirements with coordinated planned periodic purchases.

Additionally, intermixing newly purchased alloy castings along with production alloy castings, may provide for extended life for the latter.

Scrap Alloy Recycling: New Alloy Purchase Credit for Returning Your Scrap Alloy Material

When alloy castings are no longer usable in daily heat treatment operations, it can be advantageous to sell them back as scrap to the alloy supplier. The supplier should be able to provide a scrap repurchase credit that can be used for future purchases of new alloy castings.

Figure 6. Visual demonstration of capital flow for initial and subsequent alloy purchases
Source: Castalloy Group

Generally, this scrap alloy repurchase credit may be used in whole or in part as directed by the customer for new replacement alloy casting purchases.

As well as being cost-efficient, scrap alloy castings recycling supports the long-term sustainable use of metals, minimizes the potential negative impact on the earth’s environment, and reduces the overall carbon footprint of both alloy user and supplier.

Summary

Figure 7. Typical scrap alloy trays and grids
Source: Castalloy Group

To review, improving the working life of heat treating cast alloys starts with design and is maintained with factors that account for the full alloy casting life:

  • Choosing the right design and alloy composition for heat treatment castings is fundamental to optimizing their working longevity and performance. This decision can only be made by carefully considering key aspects of the intended casting
  • Maintaining furnace equipment and process environment operating conditions will also assist in maximizing the working life and overall performance of the alloy castings.
  • Alloy casting inspection will support heat treat operations and minimize potential equipment downtime by providing evidence of furnace equipment issues or malfunction.
  • Periodic budgeted alloy casting purchases support heat treat operations, will help maximize uptime, and minimize potential downtime associated with suspect or failing alloy castings.
  • Scrap (expired useful life) alloy repurchases can be used to off set the costs associated with new alloy casting purchases. Scrap alloy recycling also minimizes negative impact on the environment.

About the Author:

Matthew Fischer is the manager of Technical Sales for Heat Resistant Products at Castalloy Group NA. He has thirty years of experience in furnace design and applications working for a leading heat treat furnace equipment supplier. Additionally, he has worked for several years as a senior heat treat manufacturing engineer for a global tier-1 automotive company as well as in the controls and instrumentation fields across multiple industries, including thermal processing and heat treating.

For more information:
Contact Matthew Fischer at Matthew.Fischer@castalloygroup.com


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Formula 1 Partner Boosts Heat Treating Capabilities with Vacuum Furnace

A European subcontractor for the automotive and racing industries as well as a partner for teams participating in Formula 1 races has acquired a second vacuum furnace.

The order from SECO/WARWICK includes a Vector® vacuum furnace with 15 bar abs high pressure gas quenching, and high vacuum (HV). The furnace will process engine and gear components for vehicles racing large-scale motorsport competitions.

This partner provides carburizing, and various heat treatment services for titanium, aluminum and precipitation hardening of alloys. These services must be of aviation quality within the demanding timeframes required by European F1 teams.

In the new SECO/WARWICK furnace, the customer will execute vacuum heat treatment of titanium and its alloys and will perform vacuum carburizing processes for steel elements. Titanium alloys are very strong materials, but at the same time soft and plastic, which makes them difficult to machine. Low thermal conductivity and density creates an environment where the cutting material is subject to a strong thermal load and tends to harden.

The FIA regulations for Formula 1 racing specify in detail what material a part must consist of and how it must be manufactured. Titanium or titanium alloys are used for many engine parts and suspensions because they have high toughness, strength, and ductility, and are corrosion resistant. Formula 1 car components must be manufactured precisely and safely in both prototype and small series production.

The purpose of this particular model of Vector furnace will be unique, as carburizing and hardening of parts such as gears for engines and transmissions for high-performance F1 sports cars are not the typical processes for which SECO/WARWICK supplies its furnaces.

Commenting on this order, Maciej Korecki, vice president of the Vacuum Segment at SECO/WARWICK, explained, "The vacuum furnace system which will be delivered to England has numerous options such as cryogenic processing, convection, FineCarb® vacuum carburizing, pre-nitriding for PreNitLPC® carburizing technology or low-pressure carbonitriding LPCN."


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Fringe Friday: Airbus and Air France Propose Global MRO Venture

Sometimes our editors find items that are not exactly "heat treat" but do deal with interesting developments in one of our key markets: aerospace, automotive, medical, energy, or general manufacturing.

To celebrate getting to the “fringe” of the weekend, Heat Treat Today presents today’s Heat Treat Fringe Friday: a negotiation established between major airline players to expand maintenance capabilities.


Anne Brachet
Anne Brachet
EVP
Air France-KLM Engineering & Maintenance
Source: LinkedIn

Airbus is negotiating establishment of a new joint venture with Air France SA to provide component maintenance services (maintenance, repair, overhaul, or MRO) for the global A350 fleet. Looking at a 2024 start, the long-term maintenance needs of A350 operators will be addressed.

The Airbus A350 is a twin-engine wide-body aircraft in service on long-range routes with more than three dozen carriers and leasing agencies. According to Airbus, there are more than 550 A350 jets currently in service and more than 1,000 on order.

“This project aims to bring customers the best expertise of our two companies on a product as high-tech as the A350,” stated Anne Brachet, EVP at Air France-KLM Engineering & Maintenance.


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